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ChemicalBook CAS DataBase List Ethanethioic acid, S-(tetrahydro-1-oxido-3-thienyl) ester, (1R-cis)- (9CI)

Ethanethioic acid, S-(tetrahydro-1-oxido-3-thienyl) ester, (1R-cis)- (9CI) synthesis

1synthesis methods
Thiophene-3-ol, tetrahydro-, 4-methylbenzenesulfonate, 1-oxide, (1R-trans)- (9CI)

120788-02-5
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10387-40-3 Synthesis
Potassium thioacetate

10387-40-3
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Ethanethioic acid, S-(tetrahydro-1-oxido-3-thienyl) ester, (1R-cis)- (9CI)

120788-03-6
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Yield:120788-03-6 80%

Reaction Conditions:

in acetone;1.) reflux, 3.5 h, 2.) rt, overnight;

References:

Volkmann, Robert A.;Kelbaugh, Paul R.;Nason, Deane M.;Jasys, V. John [Journal of Organic Chemistry,1992,vol. 57,# 16,p. 4352 - 4361]