ChemicalBook CAS DataBase List Propanoic acid, 3-fluoro-2-(fluoromethyl)-2-methyl-

Propanoic acid, 3-fluoro-2-(fluoromethyl)-2-methyl- synthesis

1synthesis methods

Product Name:Propanoic acid, 3-fluoro-2-(fluoromethyl)-2-methyl-
CAS Number:1208092-05-0
Molecular formula:C5H8F2O2
Molecular Weight:138.11

179388-73-9 Synthesis

2,2-BIS-(HYDROXYMETHYL)-PROPANOIC ACID BENZYL ESTER

179388-73-9
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Propanoic acid, 3-fluoro-2-(fluoromethyl)-2-methyl-

1208092-05-0
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: diethylamino-sulfur trifluoride / dichloromethane / 12 h / -20 - 20 °C
2: hydrogen; palladium 10% on activated carbon / ethyl acetate / 12 h / 775.74 Torr

References:

US9273058,2016,B2