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3,5-DIOXO-2-[3-(TRIFLUOROMETHYL)PHENYL]-2,3,4,5-TETRAHYDRO-1,2,4-TRIAZINE-6-CARBONITRILE synthesis

2synthesis methods
ETHYL N-(2-CYANO-2-(2-[3-(TRIFLUOROMETHYL)PHENYL]HYDRAZONO)ACETYL)CARBAMATE

118806-30-7
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3,5-DIOXO-2-[3-(TRIFLUOROMETHYL)PHENYL]-2,3,4,5-TETRAHYDRO-1,2,4-TRIAZINE-6-CARBONITRILE

121065-97-2
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Yield:-

Reaction Conditions:

in 5,5-dimethyl-1,3-cyclohexadiene at 140;

References:

Rankovic, Zoran;Cai, Jiaqiang;Fradera, Xavier;Dempster, Maureen;Mistry, Ashvin;Mitchell, Ann;Long, Clive;Hamilton, Emma;King, Angela;Boucharens, Sylviane;Jamieson, Craig;Gillespie, Jonathan;Cumming, Iain;Uitdehaag, Joost;Zeeland, Mario van [Bioorganic and Medicinal Chemistry Letters,2010,vol. 20,# 5,p. 1488 - 1490] Location in patent:scheme or table