ChemicalBook CAS DataBase List Benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone, 4,5,9,10-tetrabromo-2,7-bis(2-decyltetradecyl)-

Benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone, 4,5,9,10-tetrabromo-2,7-bis(2-decyltetradecyl)- synthesis

1synthesis methods

Product Name:Benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone, 4,5,9,10-tetrabromo-2,7-bis(2-decyltetradecyl)-
CAS Number:1219501-16-2
Molecular formula:C62H98Br4N2O4
Molecular Weight:1255.07

62281-07-6
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299962-88-2 Synthesis

4,5,9,10-Tetrabromoisochromeno[6,5,4-def]isochromene-1,3,6,8- tetraone

299962-88-2
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Benzo[lmn][3,8]phenanthroline-1,3,6,8(2H,7H)-tetrone, 4,5,9,10-tetrabromo-2,7-bis(2-decyltetradecyl)-

1219501-16-2
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Yield:1219501-16-2 19%

Reaction Conditions:

Stage #1: 2-decyl-1-tetradecylamine;2,3,6,7-tetrabromonaphthalene-1,4,5,8-tetracarboxylic dianhydridewith acetic acidReflux;
Stage #2: with phosphorus tribromide in toluene;Reflux;

References:

Gao, Xike;Di, Chong-An;Hu, Yunbin;Yang, Xiaodi;Fan, Hongyu;Zhang, Feng;Liu, Yunqi;Li, Hongxiang;Zhu, Daoben [Journal of the American Chemical Society,2010,vol. 132,# 11,p. 3697 - 3699] Location in patent:supporting information; scheme or table