123990-98-7 synthesis

7synthesis methods

Product Name:123990-98-7
CAS Number:123990-98-7
Molecular formula:C13H16O2
Molecular Weight:204.26

504-02-9 Synthesis

504-02-9
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123990-98-7
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$45.00/10mg

Yield:-

Steps:

Multi-step reaction with 4 steps
1: p-toluenesulfonic acid monohydrate / toluene / 12 h / 110 °C / Molecular sieve; Dean-Stark
2: sodium tetrahydroborate / methanol / 1.5 h / 0 °C / Inert atmosphere
3: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 75 °C / Inert atmosphere
4: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 12 h / 55 °C / Inert atmosphere

References:

Beaver, Matthew G.;Buscagan, Trixia M.;Lavinda, Olga;Woerpel [Angewandte Chemie - International Edition,2016,vol. 55,# 5,p. 1816 - 1819][Angew. Chem.,2016,vol. 128,# 5,p. 1848 - 1851,4]