![](/CAS/20180808/GIF/123990-98-7.gif)
123990-98-7 synthesis
- Product Name:123990-98-7
- CAS Number:123990-98-7
- Molecular formula:C13H16O2
- Molecular Weight:204.26
![1,3-Cyclohexanedione](/CAS/GIF/504-02-9.gif)
504-02-9
553 suppliers
$5.00/10g
![123990-98-7](/CAS/20180808/GIF/123990-98-7.gif)
123990-98-7
19 suppliers
$45.00/10mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: p-toluenesulfonic acid monohydrate / toluene / 12 h / 110 °C / Molecular sieve; Dean-Stark
2: sodium tetrahydroborate / methanol / 1.5 h / 0 °C / Inert atmosphere
3: sodium hydride / tetrahydrofuran; mineral oil / 12 h / 0 - 75 °C / Inert atmosphere
4: cerium(III) chloride heptahydrate; sodium iodide / acetonitrile / 12 h / 55 °C / Inert atmosphere
References:
Beaver, Matthew G.;Buscagan, Trixia M.;Lavinda, Olga;Woerpel [Angewandte Chemie - International Edition,2016,vol. 55,# 5,p. 1816 - 1819][Angew. Chem.,2016,vol. 128,# 5,p. 1848 - 1851,4]
![2-Cyclohexen-1-one](/CAS/GIF/930-68-7.gif)
930-68-7
254 suppliers
$9.00/1g
![Benzyl alcohol](/CAS/GIF/100-51-6.gif)
100-51-6
1385 suppliers
$5.00/100g
![123990-98-7](/CAS/20180808/GIF/123990-98-7.gif)
123990-98-7
19 suppliers
$45.00/10mg
![Cyclohexanol, 3-(phenylmethoxy)-, (1R,3S)-rel-](/CAS/20210305/GIF/114737-99-4.gif)
114737-99-4
0 suppliers
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![123990-98-7](/CAS/20180808/GIF/123990-98-7.gif)
123990-98-7
19 suppliers
$45.00/10mg
![Benzene, [(3-cyclohexen-1-yloxy)methyl]-](/CAS/20210111/GIF/100611-66-3.gif)
100611-66-3
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![123990-98-7](/CAS/20180808/GIF/123990-98-7.gif)
123990-98-7
19 suppliers
$45.00/10mg
![7-Oxabicyclo[4.1.0]heptane, 3-(phenylmethoxy)-](/CAS/20210111/GIF/445481-11-8.gif)
445481-11-8
0 suppliers
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![4-(Benzyloxy)cyclohexanone](/CAS/GIF/2987-06-6.gif)
2987-06-6
89 suppliers
$11.00/1g
![123990-98-7](/CAS/20180808/GIF/123990-98-7.gif)
123990-98-7
19 suppliers
$45.00/10mg