4-MethyluMbelliferyl 3,4,6-tri-O-Acetyl-2-azido-2-deoxy-α-D-galactopyranoside synthesis
- Product Name:4-MethyluMbelliferyl 3,4,6-tri-O-Acetyl-2-azido-2-deoxy-α-D-galactopyranoside
- CAS Number:124167-43-7
- Molecular formula:C22H23N3O10
- Molecular Weight:489.44
Yield:124167-43-7 70%
Reaction Conditions:
with trimethylsilyl trifluoromethanesulfonate in dichloromethane at -20; for 8 h;Molecular sieve;Inert atmosphere;stereoselective reaction;
References:
Chang, Shih-Sheng;Lin, Chun-Cheng;Li, Yaw-Kuen;Mong, Kwok-Kong Tony [Carbohydrate Research,2009,vol. 344,# 4,p. 432 - 438] Location in patent:experimental part
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