2(3H)-Furanone, dihydro-3,4-bis[[3-methoxy-4-(phenylmethoxy)phenyl]methyl]-, (3S,4S)- synthesis

8synthesis methods

Product Name:2(3H)-Furanone, dihydro-3,4-bis[[3-methoxy-4-(phenylmethoxy)phenyl]methyl]-, (3S,4S)-
CAS Number:124988-59-6
Molecular formula:C34H34O6
Molecular Weight:538.63

2(3H)-Furanone, dihydro-4-[(4-hydroxy-3-methoxyphenyl)methyl]-, (4R)-

111266-00-3
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2(3H)-Furanone, dihydro-3,4-bis[[3-methoxy-4-(phenylmethoxy)phenyl]methyl]-, (3S,4S)-

124988-59-6
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: 90 percent / K₂CO₃, NaI / acetone / 18 h / Heating
2: 1) LHDS / 1) hexane, THF, -78 deg C, 2h, 2) THF, -78 deg C, 2 h

References:

Khamlach, Melle Kenza;Dhal, Robert;Brown, Eric [Tetrahedron,1992,vol. 48,# 46,p. 10115 - 10126]