Ethenol, 2,2-difluoro-1-(tributylstannyl)-, 1-(4-methylbenzenesulfonate) synthesis
1synthesis methods
- Product Name:Ethenol, 2,2-difluoro-1-(tributylstannyl)-, 1-(4-methylbenzenesulfonate)
- CAS Number:1256278-61-1
- Molecular formula:C21H34F2O3SSn
- Molecular Weight:523.26
Yield:1256278-62-2 94%
Reaction Conditions:
with copper(l) iodide;tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide at 80; for 10 h;Inert atmosphere;
References:
Han, Seung Yeon;Jeong, In Howa [Organic Letters,2010,vol. 12,# 23,p. 5518 - 5521] Location in patent:supporting information; experimental part