ChemicalBook CAS DataBase List 9-broMo-8-Methoxy-6,6-diMethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile

9-broMo-8-Methoxy-6,6-diMethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile synthesis

3synthesis methods

Product Name:9-broMo-8-Methoxy-6,6-diMethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile
CAS Number:1256579-03-9
Molecular formula:C20H15BrN2O2
Molecular Weight:395.25

6-broMo-7-Methoxy-1,1-diMethyl-3,4-dihydronaphthalen-2(1H)-one,

1256578-99-0
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9-broMo-8-Methoxy-6,6-diMethyl-11-oxo-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile

1256579-03-9
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: trifluoroacetic acid / 2 h / 100 °C
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water / 3 h / 0 °C

References:

Kinoshita, Kazutomo;Kobayashi, Takamitsu;Asoh, Kohsuke;Furuichi, Noriyuki;Ito, Toshiya;Kawada, Hatsuo;Hara, Sousuke;Ohwada, Jun;Hattori, Kazuo;Miyagi, Takuho;Hong, Woo-Sang;Park, Min-Jeong;Takanashi, Kenji;Tsukaguchi, Toshiyuki;Sakamoto, Hiroshi;Tsukuda, Takuo;Oikawa, Nobuhiro [Journal of Medicinal Chemistry,2011,vol. 54,# 18,p. 6286 - 6294]

1256579-00-6 Synthesis

9-broMo-8-Methoxy-6,6-diMethyl-6,11-dihydro-5H-benzo[b]carbazole-3-carbonitrile

1256579-00-6
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1256579-03-9
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References

7-Methoxy-1,1-diMethyl-3,4-dihydronaphthalen-2(1H)-one

1865-83-4
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$54.00/100mg

1256579-03-9
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References