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ChemicalBook CAS DataBase List 1256825-11-2

1256825-11-2 synthesis

1synthesis methods
321535-23-3 Synthesis
6-IODO-2,3-DIMETHOXYPYRIDINE

321535-23-3
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1256825-11-2

1256825-11-2
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: zinc(II) fluoride / tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium(0) / N,N-dimethyl-formamide / 0.5 h / 135 °C / Microwave irradiation
2.1: hydrogenchloride; hydrogen / palladium(II) hydroxide / water; methanol / 2 h
2.2: pH 9

References:

WO2011/5636,2011,A1