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126027-07-4

Carbamic acid, [(1S)-1-methyl-2-oxopropyl]-, 1,1-dimethylethyl ester (9CI) synthesis

3synthesis methods
93371-30-3 Synthesis
(S)-3-(Boc-aMino)-1-chloro-2-butanone

93371-30-3
24 suppliers
$310.00/500mg

Carbamic acid, [(1S)-1-methyl-2-oxopropyl]-, 1,1-dimethylethyl ester (9CI)

126027-07-4
8 suppliers
inquiry

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Yield:126027-07-4 95.5%

Reaction Conditions:

with hydrogen;triethylamine;palladium in methanol; pH=7 - 8; for 4 h;

References:

Miyazaki, Anna;Fujisawa, Yutaka;Shiotani, Kimitaka;Fujita, Yoshio;Li, Tingyou;Tsuda, Yuko;Yokoi, Toshio;Bryant, Sharon D.;Lazarus, Lawrence H.;Okada, Yoshio [Chemical and Pharmaceutical Bulletin,2005,vol. 53,# 9,p. 1152 - 1158]