2-(4-BENZYL-2,2-DIMETHYL-TETRAHYDRO-PYRAN-4-YL)-ETHYLAMINE synthesis

2synthesis methods

Product Name:2-(4-BENZYL-2,2-DIMETHYL-TETRAHYDRO-PYRAN-4-YL)-ETHYLAMINE
CAS Number:126318-00-1
Molecular formula:C16H25NO
Molecular Weight:247.38

(4-BENZYL-TETRAHYDRO-2,2-DIMETHYL-2H-PYRAN-4-YL)ACETIC ACID

109878-51-5
10 suppliers
$378.00/1g

2-(4-BENZYL-2,2-DIMETHYL-TETRAHYDRO-PYRAN-4-YL)-ETHYLAMINE

126318-00-1
7 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 3 steps
1: formamide, SOCl₂ / benzene / 1 h / 60 °C
2: 25percent aq. ammonia / 48 h / Ambient temperature
3: LiAlH₄ / ethanol; tetrahydrofuran / 20 h / Ambient temperature

References:

Arutyunyan, N. S.;Akopyan, L. A.;Paronikyan, R. G.;Akopyan, N. E. [Pharmaceutical Chemistry Journal,1990,vol. 24,# 5,p. 349 - 352][Khimiko-Farmatsevticheskii Zhurnal,1990,vol. 24,# 5,p. 29 - 31]