1,2-O-ISOPROPYLIDENE-3-S-HYDROXY-4-R-ETHYDINYL TETRAHYDROFURAN synthesis

3synthesis methods

Product Name:1,2-O-ISOPROPYLIDENE-3-S-HYDROXY-4-R-ETHYDINYL TETRAHYDROFURAN
CAS Number:127223-28-3
Molecular formula:C9H12O4
Molecular Weight:184.19

Dimethyl (1-Diazo-2-oxopropyl)phosphonate

90965-06-3
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53167-11-6 Synthesis

1,2-O-ISOPROPYLIDENE-ALPHA-D-XYLO-PENTODIALDO-1,4-FURANOSE

53167-11-6
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1,2-O-ISOPROPYLIDENE-3-S-HYDROXY-4-R-ETHYDINYL TETRAHYDROFURAN

127223-28-3
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Yield:127223-28-3 97%

Reaction Conditions:

Stage #1: 1,2-O-isopropylidene-α-D-xylo-pentodialdo-1,4-furanosewith potassium carbonate in methanol at 0 - 20; for 0.166667 h;
Stage #2: dimethyl 1-(1-diazo-2-oxopropyl)phosphonate in methanol at 0 - 20; for 7 h;

References:

Indu, Satrajit;Kaliappan, Krishna P.;Telore, Rahul D. [Organic and biomolecular chemistry,2020,vol. 18,# 13,p. 2432 - 2446]

α-D-Glucofuranose, 6-chloro-6-deoxy-1,2:3,5-bis-O-(1-methylethylidene)-

19685-14-4
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127223-28-3
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References

582-52-5 Synthesis

582-52-5
473 suppliers
$5.00/5g

127223-28-3
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References

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