ChemicalBook CAS DataBase List 1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene synthesis

1synthesis methods

Product Name:1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene
CAS Number:1279691-35-8
Molecular formula:C23H27ClO8
Molecular Weight:466.91

90-80-2 Synthesis

90-80-2
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1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene

1279691-35-8
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: pyridine / dichloromethane / -20 °C / Inert atmosphere; Large scale
1.2: 7 h / 10 °C / Large scale
2.1: lithium chloride; isopropylmagnesium chloride / acetonitrile / 1 h / -20 - -15 °C / Large scale
2.2: 8 h / -10 - 0 °C / Large scale

References:

Xuzhou Wan Bang Jinqiao Pharmaceutical Co., Ltd.;Jiangsu Wanbang Biochemical Pharmaceutical Group Co., Ltd.;Yuan Wei;Qiao Deshui;Dong Changqing;Gao Xueqin CN109988161, 2019, A

1-chloro-4-(β-D-glucopyranos-1-yl)-2-[4-((S)-tetrahydrofuran-3-yloxy)benzyl]benzene Related Search:

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