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(2S)-5-Oxo-2-pyrrolidinecarbothioic Acid S-Ethyl Ester synthesis

1synthesis methods
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Yield:1298024-11-9 71%

Reaction Conditions:

with dmap;dicyclohexyl-carbodiimide in dichloromethane;N,N-dimethyl-formamide at 0 - 20; for 16 h;

References:

Hoye, Adam T.;Wipf, Peter [Organic Letters,2011,vol. 13,# 10,p. 2634 - 2637] Location in patent:supporting information; experimental part