phenethyl alcohol xylopyranosyl-(1-6)-glucopyranoside synthesis
- Product Name:phenethyl alcohol xylopyranosyl-(1-6)-glucopyranoside
- CAS Number:129932-48-5
- Molecular formula:C19H28O10
- Molecular Weight:416.42
860648-07-3
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 99 percent / 4-N,N-dimethylaminopyridine (DMAP) / pyridine / 1 h / 20 °C
2: 97 percent / H2 / Pd(OH)2-C / methanol
3: 44 percent / phenylselenochloride (PhSeCl); silver triflate (AgOTf); 4 Angstroem molecular sieves / 1,2-dichloro-ethane / 1 h / 0 °C
4: 70 percent / K2CO3 / methanol / 0.5 h / 20 °C
References:
Kawahara, Eiji;Nishiuchi, Miho;Fujii, Mikio;Kato, Keisuke;Ida, Yoshiteru;Akita, Hiroyuki [Heterocycles,2005,vol. 65,# 6,p. 1461 - 1470]
192827-13-7
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129932-48-5
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132278-39-8
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860648-08-4
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2280-44-6
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129932-48-5
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