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ChemicalBook CAS DataBase List tert-Butyl 6-oxo-3-azabicyclo[3.1.1]heptane-3-carboxylate

tert-Butyl 6-oxo-3-azabicyclo[3.1.1]heptane-3-carboxylate synthesis

3synthesis methods
24424-99-5 Synthesis
Di-tert-butyl dicarbonate

24424-99-5
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6-Oxa-3-azabicyclo[3.1.1]heptane, 3-[(4-methoxyphenyl)methyl]-

1339953-54-6
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tert-Butyl 6-oxo-3-azabicyclo[3.1.1]heptane-3-carboxylate

1305208-01-8
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Yield:1305208-01-8 87%

Reaction Conditions:

with 20% palladium hydroxide on charcoal in methanol;cyclohexene; for 1.5 h;Reflux;

References:

Wishka, Donn G.;Beagley, Paul;Lyon, Jessica;Farley, Kathleen A.;Walker, Daniel P. [Synthesis,2011,# 16,art. no. M58811SS,p. 2619 - 2624] Location in patent:experimental part