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ChemicalBook CAS DataBase List 9-[2-(Diphenylphosphino)phenyl]-9H-carbazole, Min. 97% Ph PhenCar-Phos

9-[2-(Diphenylphosphino)phenyl]-9H-carbazole, Min. 97% Ph PhenCar-Phos synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: copper oxide (I); tripotassium phosphate tribasic; N,N-dimethyl-1,2-diaminoethane / toluene / 120 °C
2.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere

References:

Chun To, Sheung;Yee Kwong, Fuk [Chemical Communications,2011,vol. 47,# 17,p. 5079 - 5081]