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3-Methyl-benzo[d]isoxazole-5-boronic acid pinacol ester synthesis

4synthesis methods
66033-76-9 Synthesis
1,2-BENZISOXAZOLE, 5-BROMO-3-METHYL-

66033-76-9
48 suppliers
$85.00/250mg

3-Methyl-benzo[d]isoxazole-5-boronic acid pinacol ester

1314136-00-9
18 suppliers
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Yield:1314136-00-9 53%

Reaction Conditions:

with (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;potassium acetate in 1,4-dioxane at 80; for 15 h;Inert atmosphere;

References:

Taylor, Nicholas J.;Emer, Enrico;Preshlock, Sean;Schedler, Michael;Tredwell, Matthew;Verhoog, Stefan;Mercier, Joel;Genicot, Christophe;Gouverneur, Véronique [Journal of the American Chemical Society,2017,vol. 139,# 24,p. 8267 - 8276] Location in patent:supporting information