ChemicalBook CAS DataBase List 2-pyridinecarboxylic acid,1,6-dihydro-1-hydroxy-6-thioxo-

2-pyridinecarboxylic acid,1,6-dihydro-1-hydroxy-6-thioxo- synthesis

3synthesis methods

Product Name:2-pyridinecarboxylic acid,1,6-dihydro-1-hydroxy-6-thioxo-
CAS Number:131490-25-0
Molecular formula:C6H5NO3S
Molecular Weight:171.17

2-bromopyridine-6-carboxylic acid 1-oxide

94781-88-1
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2-pyridinecarboxylic acid,1,6-dihydro-1-hydroxy-6-thioxo-

131490-25-0
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$65.00/5mg

Yield:131490-25-0 88%

Reaction Conditions:

with sodium hydrogensulfide;sodium sulphide nonahydrate in water at 70 - 95; pH=10; for 6 h;Inert atmosphere;Reflux;

References:

Agrawal, Arpita;De Oliveira, César Augusto F.;Cheng, Yuhui;Jacobsen, Jennifer A.;McCammon, J. Andrew;Cohen, Seth M. [Journal of Medicinal Chemistry,2009,vol. 52,# 4,p. 1063 - 1074] Location in patent:experimental part

2-Bromo-6-Carboxy-1-Oxo-1,2-Dihydropyridin-1-Ium

1609646-56-1
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131490-25-0
13 suppliers
$65.00/5mg

References

21190-87-4 Synthesis

21190-87-4
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$10.00/5g

131490-25-0
13 suppliers
$65.00/5mg

References