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Di-Tert-Butyl 1-(Bicyclo[1.1.1]Pentan-1-Yl)Hydrazine-1,2-Dicarboxylate synthesis

5synthesis methods
-

Yield:1326242-72-1 99%

Reaction Conditions:

with tris(2,2,6,6-tetramethyl-3,5-heptanedionato) manganese (III);phenylsilane in diethyl ether;dichloromethane;isopropyl alcohol;pentane at 0; for 21 h;Inert atmosphere;

References:

Bunker, Kevin D.;Sach, Neal W.;Huang, Qinhua;Richardson, Paul F. [Organic Letters,2011,vol. 13,# 17,p. 4746 - 4748] Location in patent:supporting information; experimental part