1H-1,2,3-Triazole-4-carboxylic acid, 1-[(3-methoxyphenyl)methyl]- synthesis

4synthesis methods

Product Name:1H-1,2,3-Triazole-4-carboxylic acid, 1-[(3-methoxyphenyl)methyl]-
CAS Number:1340963-83-8
Molecular formula:C11H11N3O3
Molecular Weight:233.22

1-(Azidomethyl)-3-methoxybenzene (~0.5 M in MTBE)

123767-44-2
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471-25-0
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1H-1,2,3-Triazole-4-carboxylic acid, 1-[(3-methoxyphenyl)methyl]-

1340963-83-8
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Yield:1340963-83-8 88.3%

Reaction Conditions:

with bathophenanthrolinedispufonic acid disodium salt;copper(II) sulfate;sodium L-ascorbate in water;N,N-dimethyl-formamide at 0 - 20;Inert atmosphere;

References:

Bai, Suping;Li, Shihong;Xu, Jinbin;Peng, Xin;Sai, Kiran;Chu, Wenhua;Tu, Zhude;Zeng, Chenbo;Mach, Robert H. [Journal of Medicinal Chemistry,2014,vol. 57,# 10,p. 4239 - 4251] Location in patent:supporting information

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References

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1340963-83-8
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References

6971-51-3 Synthesis

6971-51-3
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References