4,4'-[(1,2,3,3,4,4-HEXAFLUOROCYCLOBUTANE-1,2-DIYL)BIS(OXY)]DIBENZOIC ACID synthesis

3synthesis methods

Product Name:4,4'-[(1,2,3,3,4,4-HEXAFLUOROCYCLOBUTANE-1,2-DIYL)BIS(OXY)]DIBENZOIC ACID
CAS Number:134151-61-4
Molecular formula:C18H10F6O6
Molecular Weight:436.26

106-41-2
484 suppliers
$13.00/5g

4,4'-[(1,2,3,3,4,4-HEXAFLUOROCYCLOBUTANE-1,2-DIYL)BIS(OXY)]DIBENZOIC ACID

134151-61-4
13 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: sodium hydroxide / water / 0.42 h
1.2: 6 h / 65 °C / 7500.75 Torr / Autoclave; Inert atmosphere
2.1: 42 h / 180 °C / 2250.23 Torr / Inert atmosphere
3.1: sodium carbonate; palladium diacetate / 1-methyl-pyrrolidin-2-one / 24 h / 120 °C / Inert atmosphere
4.1: potassium hydroxide / butan-1-ol / 4 h / Reflux

References:

WO2020/229227,2020,A1

Benzoic acid, 4-[(1,2,2-trifluoroethenyl)oxy]-

134151-66-9
25 suppliers
$40.00/100mg

134151-61-4
13 suppliers
inquiry

References

134151-77-2
12 suppliers
$179.00/250mg

134151-61-4
13 suppliers
inquiry

References