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2-Bromo-5-butyl-4H-thieno[2,3-c]pyrrole-4,6(5H)-dione synthesis

3synthesis methods
4H-Thieno[2,3-c]pyrrole-4,6(5H)-dione, 5-butyl-

1350462-23-5
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2-Bromo-5-butyl-4H-thieno[2,3-c]pyrrole-4,6(5H)-dione

1350462-24-6
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Yield:1350462-24-6 78%

Reaction Conditions:

with N-Bromosuccinimide;sulfuric acid;trifluoroacetic acid in water at 20;

References:

Melucci, Manuela;Zambianchi, Massimo;Favaretto, Laura;Gazzano, Massimo;Zanelli, Alberto;Monari, Magda;Capelli, Raffaella;Troisi, Stefano;Toffanin, Stefano;Muccini, Michele [Chemical Communications,2011,vol. 47,# 43,p. 11840 - 11842] Location in patent:supporting information; experimental part