ChemicalBook CAS DataBase List 5-Amino-2-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

5-Amino-2-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile synthesis

3synthesis methods

Product Name:5-Amino-2-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile
CAS Number:1350635-52-7
Molecular formula:C13H17BN2O2
Molecular Weight:244.1

5-Nitro-2-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

1565857-68-2
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5-Amino-2-(tetramethyl-1,3,2-dioxaborolan-2-yl)benzonitrile

1350635-52-7
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Yield:1350635-52-7 73%

Reaction Conditions:

with 5%-palladium/activated carbon;hydrogen in methanol at 20; under 760.051 Torr; for 4 h;

References:

Qiu, Di;Wang, Shuai;Tang, Shengbo;Meng, He;Jin, Liang;Mo, Fanyang;Zhang, Yan;Wang, Jianbo [Journal of Organic Chemistry,2014,vol. 79,# 5,p. 1979 - 1988]