ChemicalBook CAS DataBase List 4,4',5,5'-tetra(pyridin-3-yl)-2,2'-bi(1,3-dithiolylidene)

4,4',5,5'-tetra(pyridin-3-yl)-2,2'-bi(1,3-dithiolylidene) synthesis

1synthesis methods

Product Name:4,4',5,5'-tetra(pyridin-3-yl)-2,2'-bi(1,3-dithiolylidene)
CAS Number:1356336-68-9
Molecular formula:C26H16N4S4
Molecular Weight:512.69

626-55-1 Synthesis

626-55-1
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31366-25-3 Synthesis

31366-25-3
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$53.00/200mg

4,4',5,5'-tetra(pyridin-3-yl)-2,2'-bi(1,3-dithiolylidene)

1356336-68-9
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Yield:1356336-68-9 60%

Reaction Conditions:

with palladium diacetate;caesium carbonate;tri tert-butylphosphoniumtetrafluoroborate in 1,4-dioxane; for 24 h;Inert atmosphere;Reflux;

References:

Vajpayee, Vaishali;Bivaud, Sebastien;Goeb, Sebastien;Croue, Vincent;Allain, Magali;Popp, Brian V.;Garci, Amine;Therrien, Bruno;Salle, Marc [Organometallics,2014,vol. 33,# 7,p. 1651 - 1658]