8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE synthesis

1synthesis methods

Product Name:8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE
CAS Number:135692-39-6
Molecular formula:C13H13NOS3
Molecular Weight:295.44

6-METHOXY-2,2,4-TRIMETHYL-1,2-DIHYDROQUINOLINE

4053-50-3
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8-METHOXY-4,4-DIMETHYL-4,5-DIHYDRO-1H-[1,2]DITHIOLO[3,4-C]QUINOLINE-1-THIONE

135692-39-6
11 suppliers
$158.00/500mg

Yield:135692-39-6 52%

Reaction Conditions:

with sulfur in N,N-dimethyl-formamide; for 8 h;Heating;

References:

Ozhogina, O. A.;Gol'dfein, M. D.;Chumaevskii, N. B.;Shikhaliev, Kh. S.;Shmyreva, Zh. V.;Rozantsev, E. G. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1991,vol. 40,# 4.1,p. 684 - 687][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1991,# 4,p. 782 - 786]