4,4',4"-boranetriyltris(2,3,5,6-tetramethylbenzoic acid) synthesis
- Product Name:4,4',4"-boranetriyltris(2,3,5,6-tetramethylbenzoic acid)
- CAS Number:1358822-48-6
- Molecular formula:C33H39BO6
- Molecular Weight:542.47
124-38-9
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321735-68-6
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1358822-48-6
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Yield:1358822-48-6 87%
Reaction Conditions:
Stage #1: tris(4-bromo-2,3,5,6-tetramethylphenyl)boranewith n-butyllithium in tetrahydrofuran at -78 - -60; for 1 h;Inert atmosphere;
Stage #2: carbon dioxide in tetrahydrofuran; for 1 h;Inert atmosphere;
References:
Shyshkanov, Serhii;Nguyen, Tu N.;Ebrahim, Fatmah Mish;Stylianou, Kyriakos C.;Dyson, Paul J. [Angewandte Chemie - International Edition,2019,vol. 58,# 16,p. 5371 - 5375][Angew. Chem.,2019,vol. 131,# 16,p. 5425 - 5429,5] Location in patent:supporting information
95-93-2
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1358822-48-6
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