ChemicalBook CAS DataBase List 1-benzyl-3-chloroMethylazetidine-3-carboxylic acid ethyl ester

1-benzyl-3-chloroMethylazetidine-3-carboxylic acid ethyl ester synthesis

8synthesis methods

Product Name:1-benzyl-3-chloroMethylazetidine-3-carboxylic acid ethyl ester
CAS Number:137266-85-4
Molecular formula:C14H18ClNO2
Molecular Weight:267.75

64-17-5 Synthesis

64-17-5
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1-benzyl-3,3-bis(chloromethyl)azetidin-2-one

137266-59-2
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1-benzyl-3-chloroMethylazetidine-3-carboxylic acid ethyl ester

137266-85-4
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Yield:137266-85-4 60 g

Reaction Conditions:

Stage #1: ethanol;1-benzyl-3,3-bis(chloromethyl)azetidin-2-onewith sodium at 20; for 14 h;
Stage #2: with potassium carbonate in toluene; for 16 h;Heating;Further stages.;

References:

Stocks, Michael J.;Hamza, Daniel;Pairaudeau, Garry;Stonehouse, Jeffrey P.;Thorne, Philip V. [Synlett,2007,# 16,p. 2587 - 2589]

141-52-6 Synthesis

141-52-6
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137266-59-2
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137266-85-4
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References

3-CHLORO-2,2-DICHLOROMETHYL PROPIONIC ACID

17831-70-8
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137266-85-4
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References

3-chloro-2,2-bis(chloromethyl)propanoyl chloride

50547-79-0
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137266-85-4
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References

N-benzyl-3-chloro-2,2-bis(chloromethyl)propanamide

137606-01-0
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137266-85-4
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References