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ChemicalBook CAS DataBase List 4-Chloro-2-(trifluoroMethyl)thieno[2,3-d]pyriMidine

4-Chloro-2-(trifluoroMethyl)thieno[2,3-d]pyriMidine synthesis

2synthesis methods
Thieno[2,3-d]pyrimidin-4(1H)-one, 2-(trifluoromethyl)-

1374831-01-2
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4-Chloro-2-(trifluoroMethyl)thieno[2,3-d]pyriMidine

1374831-02-3
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Yield:1374831-02-3 73%

Reaction Conditions:

with trichlorophosphate at 90; for 0.3 h;Microwave irradiation;

References:

Song, Xin Jian;Duan, Zheng Chao;Shao, Yu;Dong, Xing Gao [Chinese Chemical Letters,2012,vol. 23,# 5,p. 549 - 552] Location in patent:experimental part