[(6AR,10AR)-1-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-3-(1,1-DIMETHYL-HEPTYL)-6,6-DIMETHYL-6A,7,10,10A-TETRAHYDRO-6H-BENZO[C]CHROMEN-9-YL]-METHANOL synthesis

3synthesis methods

Product Name:[(6AR,10AR)-1-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-3-(1,1-DIMETHYL-HEPTYL)-6,6-DIMETHYL-6A,7,10,10A-TETRAHYDRO-6H-BENZO[C]CHROMEN-9-YL]-METHANOL
CAS Number:137945-53-0
Molecular formula:C31H52O3Si
Molecular Weight:500.83

2,2-DIMETHYL-PROPIONIC ACID (6AR,10AR)-1-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-3-(1,1-DIMETHYL-HEPTYL)-6,6-DIMETHYL-6A,7,10,10A-TETRAHYDRO-6H-BENZO[C]CHROMEN-9-YLMETHYL ESTER

137945-54-1
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[(6AR,10AR)-1-(TERT-BUTYL-DIMETHYL-SILANYLOXY)-3-(1,1-DIMETHYL-HEPTYL)-6,6-DIMETHYL-6A,7,10,10A-TETRAHYDRO-6H-BENZO[C]CHROMEN-9-YL]-METHANOL

137945-53-0
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Yield:137945-53-0 67%

Reaction Conditions:

with lithium aluminium tetrahydride in diethyl ether; for 1.5 h;Heating;

References:

Burstein, Sumner H.;Audette, Charlene A.;Breuer, Aviva;Devane, William A.;Colodner, Sharona;et al. [Journal of Medicinal Chemistry,1992,vol. 35,# 17,p. 3135 - 3141]

2,2-DiMethyl-propanoic Acid (6aR-trans)-[3-(1,1-DiMethylheptyl)-6a,7,10,10a-tetrahydro-1-hydroxy-6,6-diMethyl-6H-dibenzo[b,d]pyran-9-yl]Methyl Ester

113418-02-3
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References

18162-48-6 Synthesis

18162-48-6
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References