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ChemicalBook CAS DataBase List (R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide

(R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide synthesis

3synthesis methods
73295-12-2 Synthesis
(2S)-2,3-DIMETHYLBUTANE-1,3-DIOL

73295-12-2
21 suppliers
$165.00/50mg

(R)-(3-hydroxy-2,3-diMethylbutyl)triphenylphosphoniuM iodide

138079-59-1
11 suppliers
inquiry

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 98 percent / pyridine / 14 h / -4 °C
2: 85 percent / LiI / tetrahydrofuran / 0.25 h / Heating
3: 100 percent / acetonitrile / 40 h / Heating

References:

Hanekamp;Rookhuizen Boer;Bos;Brandsma [Tetrahedron,1992,vol. 48,# 24,p. 5151 - 5162]