ChemicalBook CAS DataBase List 2-Pyridinemethanamine,alpha-(1-methylethyl)-,(alphaR)-(9CI)

2-Pyridinemethanamine,alpha-(1-methylethyl)-,(alphaR)-(9CI) synthesis

3synthesis methods

Product Name:2-Pyridinemethanamine,alpha-(1-methylethyl)-,(alphaR)-(9CI)
CAS Number:138175-25-4
Molecular formula:C9H14N2
Molecular Weight:150.22

59576-30-6
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2-Pyridinemethanamine,alpha-(1-methylethyl)-,(alphaR)-(9CI)

138175-25-4
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 30 percent / Ti(OEt)4 / tetrahydrofuran / 72 h / 70 °C
2.1: NaBH₄ / methanol / 1 h / 25 °C
2.2: aq. HCl / methanol / 20 °C

References:

Chelucci, Giorgio;Baldino, Salvatore;Chessa, Simona;Pinna, Gerard A.;Soccolini, Franco [Tetrahedron Asymmetry,2006,vol. 17,# 22,p. 3163 - 3169]

3731-51-9 Synthesis

3731-51-9
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138175-25-4
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References

Bicyclo[3.1.1]heptan-2-ol, 2,6,6-trimethyl-3-[(2-pyridinylmethyl)imino]-, (1S,2S,3Z,5S)-

323584-20-9
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138175-25-4
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References

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2-Pyridinemethanamine,alpha-ethyl-,(alphaR)-(9CI) 2-Pyridinemethanamine,alpha-ethyl-(9CI)