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ChemicalBook CAS DataBase List 9-[4'-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)[1,1'-BIPHENYL]-3-YL]-9H-CARBAZOLE

9-[4'-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)[1,1'-BIPHENYL]-3-YL]-9H-CARBAZOLE synthesis

2synthesis methods
864377-33-3 Synthesis
3-(9H-Carbazol-9-yl)phenylboronic acid

864377-33-3
217 suppliers
$8.00/250mg

9-[4'-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)[1,1'-BIPHENYL]-3-YL]-9H-CARBAZOLE

1385826-87-8
24 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 12 h / Reflux
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; tricyclohexylphosphine / N,N-dimethyl-formamide / 12 h / Reflux

References:

Samsung SDI Co., Ltd;Shin Chang-ju;Kim Chang-u;Kim Hyeong-seon;Ryu Dong-wan;Lee Seung-jae;Lee Han-il;Jeong Ho-guk;Ryu Jin-hyeon;Park Seung-in;Ryu Dong-gyu;Jeong Seong-hyeon KR102031300, 2019, B1