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1,3,2-Dioxaborolane, 2-[2,4-bis(hexyloxy)phenyl]-4,4,5,5-tetraMethyl- synthesis

4synthesis methods
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Yield:1391734-70-5 70%

Reaction Conditions:

with tris-(dibenzylideneacetone)dipalladium(0);sodium acetate;XPhos in 1,4-dioxane at 95; for 10 h;Inert atmosphere;

References:

Yum, Jun-Ho;Holcombe, Thomas W.;Kim, Yongjoo;Yoon, Junghyun;Rakstys, Kasparas;Nazeeruddin, Mohammad K.;Graetzel, Michael [Chemical Communications,2012,vol. 48,# 87,p. 10727 - 10729] Location in patent:supporting information