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ChemicalBook CAS DataBase List (1α,3R,4α,5R)-3,5-Bis[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1-hydroxy-4-(1H-iMidazol-1-ylthioxoMethoxy)-cyclohexanecarboxylic Acid Methyl Ester

(1α,3R,4α,5R)-3,5-Bis[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1-hydroxy-4-(1H-iMidazol-1-ylthioxoMethoxy)-cyclohexanecarboxylic Acid Methyl Ester synthesis

3synthesis methods
135711-62-5 Synthesis
(1α,3R,4α,5R)-3,5-Bis[[(1,1-diMethylethyl)diMethylsilyl]oxy]-1,4-dihydroxy-cyclohexanecarboxylic Acid Methyl Ester

135711-62-5
9 suppliers
$150.00/25mg

6160-65-2 Synthesis
1,1'-Thiocarbonyldiimidazole

6160-65-2
406 suppliers
$6.00/1g

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Yield:139356-32-4 91%

Reaction Conditions:

in dichloromethane; for 60 h;Ambient temperature;

References:

Perlman, Kato L.;Swenson, Rolf E.;Paaren, Herbert E.;Schnoes, Heinrich K.;DeLuca, Hector F. [Tetrahedron Letters,1991,vol. 32,# 52,p. 7663 - 7666]