ChemicalBook CAS DataBase List 2-ACETAMIDO-1,3-DI-O-BENZYL-4,6-O-BENZYLIDENE-2-DEOXY-B-D-GLUCOPYRANOSIDE

2-ACETAMIDO-1,3-DI-O-BENZYL-4,6-O-BENZYLIDENE-2-DEOXY-B-D-GLUCOPYRANOSIDE synthesis

1synthesis methods

Product Name:2-ACETAMIDO-1,3-DI-O-BENZYL-4,6-O-BENZYLIDENE-2-DEOXY-B-D-GLUCOPYRANOSIDE
CAS Number:14040-20-1
Molecular formula:C29H31NO6
Molecular Weight:489.56

β-D-Glucopyranoside, phenylmethyl 2-(benzoylamino)-2-deoxy-4,6-O-(phenylmethylene)-3-O-2-propen-1-yl-

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2-ACETAMIDO-1,3-DI-O-BENZYL-4,6-O-BENZYLIDENE-2-DEOXY-B-D-GLUCOPYRANOSIDE

14040-20-1
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$200.00/100mg

Yield:-

Steps:

Multi-step reaction with 7 steps
1: sodium hydride / dimethylformamide
2: lithium aluminium hydride / diethyl ether / Ambient temperature
3: pyridinium p-toluenesulphonate / H₂O; pyridine / Ambient temperature
4: pyridine
5: mercuric chloride-mercuric oxide
6: sodium hydride / dimethylformamide
7: potassium tert-butoxide / dimethylsulfoxide / Ambient temperature

References:

Gigg, Roy;Conant, Robert [Carbohydrate Research,1982,vol. 100,p. C5 - C9]

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