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2-Azidoethyl 2,3,4,6-tetra-O-acetyl-alpha-D-mannopyranoside synthesis

7synthesis methods
849420-02-6 Synthesis
2-Chloroethyl-2,3,4,6-tetra-O-acetyl-a-D-mannopyranoside

849420-02-6
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 2-Azidoethyl 2,3,4,6-tetra-O-acetyl-alpha-D-mannopyranoside

140428-83-7
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Yield:140428-83-7 95.3%

Reaction Conditions:

with sodium azide in N,N-dimethyl-formamide at 50; for 72 h;

References:

Zhao, Yuyan;Tram, Kha;Yan, Hongbin [Carbohydrate Research,2009,vol. 344,# 16,p. 2137 - 2143] Location in patent:experimental part