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Ethyl5-(aminomethyl)-2-(difluoromethyl)pyridine-4-carboxylate synthesis
- Product Name:Ethyl5-(aminomethyl)-2-(difluoromethyl)pyridine-4-carboxylate
- CAS Number:1415206-83-5
- Molecular formula:C10H12F2N2O2
- Molecular Weight:230.21
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: acetic anhydride / 12 h / 100 °C
2.1: N,N-dimethyl-formamide / 5 h / 65 °C
2.2: 12 h / Heating
3.1: triethylamine; hydrogen; palladium 10% on activated carbon / ethanol / 2 h / 2068.65 Torr
4.1: hydrogenchloride / ethanol / 2 h / 22 - 26 °C
References:
US2013/210844,2013,A1
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