3,9-Diazabicyclo[3.3.1]nonan-7-one,3,9-dimethyl-,oxime(9CI) synthesis

2synthesis methods

Product Name:3,9-Diazabicyclo[3.3.1]nonan-7-one,3,9-dimethyl-,oxime(9CI)
CAS Number:141549-87-3
Molecular formula:C9H17N3O
Molecular Weight:0

(2E,2E)-dimethyl 4,4-(methylazanediyl)bis(but-2-enoate)(WXG01673)

852052-29-0
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3,9-Diazabicyclo[3.3.1]nonan-7-one,3,9-dimethyl-,oxime(9CI)

141549-87-3
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 73 percent / methanol / 0 - 25 °C
2: t-BuOK / toluene / Heating
3: aq HCl / Heating
4: 72 percent / NH₂OH*HCl, K₂CO₃ / ethanol / Heating

References:

Gregory, J. A.;Jennings, A. J.;Joiner, G. F.;King, F. D.;Rahman, S. K. [Tetrahedron Letters,1995,vol. 36,# 1,p. 155 - 158]

(1R)-3,9-dimethyl-3,9-diazabicyclo[3.3.1]nonan-7-one(WXG01674)

141549-84-0
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141549-87-3
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References