1,3-Cyclopentadiene-1,3-dicarboxylic acid, 2,4-dimethyl-5-[[tris(1-methylethyl)silyl]methylene]-, 1,3-diethyl ester synthesis

5synthesis methods

Product Name:1,3-Cyclopentadiene-1,3-dicarboxylic acid, 2,4-dimethyl-5-[[tris(1-methylethyl)silyl]methylene]-, 1,3-diethyl ester
CAS Number:1417407-35-2
Molecular formula:C23H38O4Si
Molecular Weight:406.63

4341-76-8 Synthesis

4341-76-8
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1,3-Cyclopentadiene-1,3-dicarboxylic acid, 2,4-dimethyl-5-[[tris(1-methylethyl)silyl]methylene]-, 1,3-diethyl ester

1417407-35-2
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere
2: bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate / 1,4-dioxane / 16 h / 80 °C / Inert atmosphere

References:

Shibata, Yu;Tanaka, Ken [Angewandte Chemie - International Edition,2011,vol. 50,# 46,p. 10917 - 10921]

4341-76-8 Synthesis

4341-76-8
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89343-06-6 Synthesis