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(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide synthesis
- Product Name:(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide
- CAS Number:1417997-93-3
- Molecular formula:C22H19NO3
- Molecular Weight:345.39
![7-Methoxycoumarin](/CAS/GIF/531-59-9.gif)
531-59-9
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$5.00/25mg
![(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide](/CAS/20180527/GIF/1417997-93-3.gif)
1417997-93-3
64 suppliers
$35.00/1mg
Yield:-
Steps:
Multi-step reaction with 6 steps
1: 6 h / Inert atmosphere
2: pyridine / dichloromethane / 2 h / 20 °C
3: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C
4: lithium hydroxide / methanol
5: triethylamine / tetrahydrofuran / 1 h / 20 °C
6: hydroxylamine hydrochloride; potassium hydroxide / methanol / 3 h / 20 °C
References:
Huang, Wei-Jan;Wang, Yi-Ching;Chao, Shi-Wei;Yang, Chen-Yui;Chen, Liang-Chieh;Lin, Mei-Hsiang;Hou, Wen-Chi;Chen, Mei-Yu;Lee, Tai-Lin;Yang, Ping;Chang, Chung-I [ChemMedChem,2012,vol. 7,# 10,p. 1815 - 1824]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide](/CAS/20180527/GIF/1417997-93-3.gif)
1417997-93-3
64 suppliers
$35.00/1mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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![(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide](/CAS/20180527/GIF/1417997-93-3.gif)
1417997-93-3
64 suppliers
$35.00/1mg
![2-Propenoic acid, 3-(2-hydroxy-4-methoxyphenyl)-, ethyl ester, (E)-](/CAS/20180601/GIF/139386-27-9.gif)
139386-27-9
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![(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide](/CAS/20180527/GIF/1417997-93-3.gif)
1417997-93-3
64 suppliers
$35.00/1mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
0 suppliers
inquiry
![(E)-N-hydroxy-4-methoxy-2-(biphenyl-4-yl)cinnamamide](/CAS/20180527/GIF/1417997-93-3.gif)
1417997-93-3
64 suppliers
$35.00/1mg