1-(2-BROMO-4-METHYLPHENYL)-1H-PYRROLE-2-CARBALDEHYDE synthesis
- Product Name:1-(2-BROMO-4-METHYLPHENYL)-1H-PYRROLE-2-CARBALDEHYDE
- CAS Number:142045-46-3
- Molecular formula:C12H10BrNO
- Molecular Weight:264.12
583-68-6
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142045-46-3
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 80 percent / acetic acid / 1,2-dichloro-ethane; H2O / 80 °C
2.1: phosphorus oxychloride / 0.17 h / -10 °C
2.2: 63 percent / 1,2-dichloro-ethane / 3 h / 100 °C
References:
Hulcoop, David G.;Lautens, Mark [Organic Letters,2007,vol. 9,# 9,p. 1761 - 1764]