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4-bromo-2,5-dimethylbenzenesulfonyl chloride(SALTDATA: FREE) synthesis

1synthesis methods
-

Yield:14207-30-8 90%

Reaction Conditions:

with chlorosulfonic acid in chloroform at 0 - 20; for 4.5 h;

References:

Pizzolato, Stefano F.;Collins, Beatrice S. L.;van Leeuwen, Thomas;Feringa, Ben L. [Chemistry - A European Journal,2017,vol. 23,# 25,p. 6174 - 6184] Location in patent:supporting information