Benzothiazole, 2-[[phenyl(phenylazo)methylene]hydrazino]-, (Z,E)- (9CI) synthesis
- Product Name:Benzothiazole, 2-[[phenyl(phenylazo)methylene]hydrazino]-, (Z,E)- (9CI)
- CAS Number:142399-45-9
- Molecular formula:C20H15N5S
- Molecular Weight:357.43
100-34-5
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100-52-7
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$21.30/2g
615-21-4
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$45.00/10mg
142399-45-9
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Yield:142399-45-9 45%
Reaction Conditions:
Stage #1: benzaldehyde;1,3-benzothiazol-2-ylhydrazinewith acetic acid in methanol at 20; for 1 h;
Stage #2: with sodium acetate;sodium hydroxide at 20;
Stage #3: benzene diazonium chloride in water at 0; for 4 h;
References:
Boyle, Paul D.;Buguis, Francis L.;Gilroy, Joe B. [Dyes and Pigments,2022,vol. 198,art. no. 110002]
