tert-butyl N-[3-[methoxy(methyl)amino]-3-oxopropyl]carbamate synthesis
- Product Name:tert-butyl N-[3-[methoxy(methyl)amino]-3-oxopropyl]carbamate
- CAS Number:142570-56-7
- Molecular formula:C10H20N2O4
- Molecular Weight:232.28
3303-84-2
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$6.00/5g
6638-79-5
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142570-56-7
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$45.00/50mg
Yield:142570-56-7 100%
Reaction Conditions:
Stage #1: N-tert-butoxycarbonyl-β-alaninewith 4-methyl-morpholine;isobutyl chloroformate in dichloromethane at -15; for 0.25 h;
Stage #2: O,N-dimethyl-hydroxylamine hydrochloride in dichloromethane at -15 - 20; for 16 h;
References:
Blaney, Paul;Grigg, Ronald;Rankovic, Zoran;Thornton-Pett, Mark;Xu, Juan [Tetrahedron,2002,vol. 58,# 9,p. 1719 - 1737]