METHYL 3-BROMO-6-METHYLTHIENO[2,3-B]PYRIDINE-2-CARBOXYLATE synthesis

2synthesis methods

Product Name:METHYL 3-BROMO-6-METHYLTHIENO[2,3-B]PYRIDINE-2-CARBOXYLATE
CAS Number:1427420-48-1
Molecular formula:C10H8BrNO2S
Molecular Weight:286.14

Thieno[2,3-b]pyridine-2-carboxylic acid, 3-aMino-6-Methyl-, Methyl ester

193400-52-1
27 suppliers
$117.00/1g

METHYL 3-BROMO-6-METHYLTHIENO[2,3-B]PYRIDINE-2-CARBOXYLATE

1427420-48-1
6 suppliers
inquiry

Yield:1427420-48-1 56%

Reaction Conditions:

with tert.-butylnitrite;copper(ll) bromide in acetonitrile at 65; for 2 h;Inert atmosphere;

References:

Romagnoli, Romeo;Baraldi, Pier Giovanni;Kimatrai Salvador, Maria;Preti, Delia;Aghazadeh Tabrizi, Mojgan;Bassetto, Marcella;Brancale, Andrea;Hamel, Ernest;Castagliuolo, Ignazio;Bortolozzi, Roberta;Basso, Giuseppe;Viola, Giampietro [Journal of Medicinal Chemistry,2013,vol. 56,# 6,p. 2606 - 2618] Location in patent:supporting information

28900-10-9 Synthesis

2-Chloro-6-methyl-3-pyridinecarbonitrile

28900-10-9
236 suppliers
$9.00/1g

1427420-48-1
6 suppliers
inquiry

References