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ChemicalBook CAS DataBase List Pyridine, 4,4'-[2-(trifluoromethyl)-1,4-phenylene]bis-

Pyridine, 4,4'-[2-(trifluoromethyl)-1,4-phenylene]bis- synthesis

1synthesis methods
7657-09-2 Synthesis
2,5-DIBROMOBENZOTRIFLUORIDE

7657-09-2
142 suppliers
$8.00/5g

1692-15-5 Synthesis
Pyridine-4-boronic acid

1692-15-5
444 suppliers
$6.00/1g

Pyridine, 4,4'-[2-(trifluoromethyl)-1,4-phenylene]bis-

1429342-61-9
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Yield:1429342-61-9 1.0 mmol

Reaction Conditions:

with potassium phosphate;tris-(dibenzylideneacetone)dipalladium(0);tricyclohexylphosphine in 1,4-dioxane;water at 100; for 18 h;Inert atmosphere;Schlenk technique;Suzuki Coupling;

References:

Culp, Jeffrey T.;Madden, Catherine;Kauffman, Kristi;Shi, Fan;Matranga, Christopher [Inorganic Chemistry,2013,vol. 52,# 8,p. 4205 - 4216] Location in patent:supporting information