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3-Morpholinone, 4-(phenylmethyl)-5-(trifluoromethyl)-, (5R)- synthesis
- Product Name:3-Morpholinone, 4-(phenylmethyl)-5-(trifluoromethyl)-, (5R)-
- CAS Number:1430086-51-3
- Molecular formula:C12H12F3NO2
- Molecular Weight:259.22
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: triethylamine; triphenylphosphine / tetrachloromethane; acetonitrile / 24 h
2: sulfuric acid / water / 24 h
3: triethylamine / dichloromethane / 48 h / Cooling with ice
4: potassium carbonate / methanol; water / 15 h / Reflux
References:
Shcherbatiuk, Andriy V.;Shyshlyk, Oleg S.;Yarmoliuk, Dmytro V.;Shishkin, Oleg V.;Shishkina, Svitlana V.;Starova, Viktoriia S.;Zaporozhets, Olga A.;Zozulya, Sergey;Moriev, Roman;Kravchuk, Olga;Manoilenko, Olga;Tolmachev, Andrey A.;Mykhailiuk, Pavel K. [Tetrahedron,2013,vol. 69,# 19,p. 3796 - 3804]
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