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ChemicalBook CAS DataBase List 1-Piperidinecarboxylic acid, 4-[1-(2-phenyl-1H-benziMidazol-1-yl)-2-[4-[1-(phenylMethyl)-1H-benziMidazol-2-yl]phenoxy]ethyl]-, 1,1-diMethylethyl ester

1-Piperidinecarboxylic acid, 4-[1-(2-phenyl-1H-benziMidazol-1-yl)-2-[4-[1-(phenylMethyl)-1H-benziMidazol-2-yl]phenoxy]ethyl]-, 1,1-diMethylethyl ester synthesis

10synthesis methods
1-Piperidinecarboxylic acid, 4-[2-[[(1,1-diMethylethoxy)carbonyl](phenylMethyl)aMino]-2-oxo-1-(2-phenyl-1H-benziMidazol-1-yl)ethyl]-, 1,1-diMethylethyl ester

1440753-63-8
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1-Piperidinecarboxylic acid, 4-[1-(2-phenyl-1H-benziMidazol-1-yl)-2-[4-[1-(phenylMethyl)-1H-benziMidazol-2-yl]phenoxy]ethyl]-, 1,1-diMethylethyl ester

1440754-07-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 15 h / 20 °C
2: hydrogenchloride / dichloromethane; 1,4-dioxane

References:

Zimmermann, Gunther;Schultz-Fademrecht, Carsten;Küchler, Philipp;Murarka, Sandip;Ismail, Shehab;Triola, Gemma;Nussbaumer, Peter;Wittinghofer, Alfred;Waldmann, Herbert [Journal of Medicinal Chemistry,2014,vol. 57,# 12,p. 5435 - 5448]